°</sup>C )及消解時間(20、30、 40min )進行優(yōu)化,篩選最優(yōu)消解條件。調(diào)整光源電流、狹縫寬度、燃氣流速、石墨爐升溫速率及背景校正模式,優(yōu)化儀器檢測參數(shù)。結(jié)果:HNO3-HF-HCI體系在消解溫度為 200<sup>°</sup>C 和消解時間為 40min 的條件下,更能提高食品中重金屬檢測精度。調(diào)整光源電流至 8mA 、狹縫寬度至 0.5nm 、燃氣流速至 2.0L?min<sup>-1</sup> 、石墨爐升溫速率至 15<sup>°</sup>C?s<sup>-1</sup> ,并采用塞曼效應(yīng)校正后,檢測靈敏度可提高 5.32%~9.87% 。結(jié)論:優(yōu)化后的方法能夠有效提高食品安全檢測可靠性,為食品重金屬污染監(jiān)測提供科學依據(jù)。-龍源期刊網(wǎng)" />

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基于原子吸收光譜法的食品中重金屬檢測方法優(yōu)化研究

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Optimization of Heavy Metal Detection Method in Food Based on Atomic Absorption Spectrometry

JIANG Yan

(Lianjian (Shandong) Technology Co.,Ltd.,Yantai 26410o, China)

Abstract: Objective: To optimize the detection method of heavy metals in food based on atomic absorption spectrometryto ensure the scientific monitoring offood safety. Method: Different substrates,acid systems,digestion temperature (150,180, 200°C ) and digestion time (20,30,40 min) were used to optimize the digestion conditions. Adjust the light source current, slit width,gas flow rate,graphite furnace heating rate and background correction mode,optimize the instrument detection parameters. Result: The digestion temperature of HNO3 -HF-HCl system is 200°C and the digestion time is 40min ,which can improve the detection accuracy of heavy metals in food.After adjusting the light source current to 8mA , slit width to 0.5nm , gas flow rate to 2.0L?min-1 ,graphite furnace heating rate to 15°C?s-1 ,and using Zeeman effect correction, the detection sensitivity can be increased by 5.32% to 9.87% Conclusion: The optimized method can efectively improve the reliability of food safety detection and provide scientific basis for food heavy metal pollution monitoring.

Keywords: atomic absorption spectrometry; food safety; heavy metal detection

食品中重金屬污染嚴重威脅消費者健康,長期攝入重金屬超標的食品會導致神經(jīng)毒性、腎損傷及致癌風險[1]。(剩余3098字)

目錄
monitor